Sunday, August 2, 2009

Measure the absortances of trie two solutions at about 287 nm and at about 450 nm

Afcsortiance of both solutions at about 287 nm is not more than 0 15 and at about 450 nm is not more than 0.03, Appendix 5.5 Heavy metals Not more than 10 ppm, determined on 1.0 g by MethodB. Appendix 3,12 Suiphated ash: Not more than 0.1 %, Appendix 3.22.Loss on drying Not more than 0.5%, determined on 1 g by drying in an oven at 105°. Appendix 8.6 Assay Weigh accurately about 0.2 g. dissolve in about 100 ml of anhydrous glacial acebc acid with gentle heat to effect solution, cool and carry out Method B for non-aqueous tilration. Appendix 3.45, using crystal violet 'solution as indicator Perform a blank determination and make any necessary correction Each ml of 0.1M perchlonc acid is equivalent to 0.01312 g of C6 H13 NO2 iAMINOCAPRQIC ACID INJECTION Aminocaproic Acid Injection is a sterile solution of Aminocaproic Acifl in Water for Injection.Usual strength 400-mg per ml. STANDARDSAminocaproic Acid Injection contains not less than 92.5 per cent and not more than 1075 per cent of the staled amount of aminocaproic acid, CftH]3NO? Identification To a volume equivalent to 0.4 g of Ammocaproic Acid add 1 ml of ether, stir, add 2 ml of

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